Effective January 1, 2019
GLP Price List
Physical / Chemical Properties (includes protocols, QA, and reports)
| Odor / Color (OPPTS 830.6302 and 6304) |
400 |
| Physical State (OPPTS 830.6303) |
400 |
| pH (OPPTS 830.7000) |
475 |
| Viscosity (OPPTS 830.7100) |
1,000 |
| Density (OPPTS 830.7300) |
750 |
| Flammability (OPPTS 830.6315) |
860 |
| Oxidation / Reduction (OPPTS 830.6314) |
1,650 |
| UV – Visible Spectrum (OPPTS 830.7050) |
1,625 |
| Melting Point (OPPTS 830.7200) |
575 |
| Boiling Point (OPPTS 830.7220) |
1,050 |
Storage Stability / Corrosion (OPPTS 630.6317 and 6320)
| 1 – year Stability – 1 Active by HPLC or GC |
9,500 |
| 1 – year Stability – 2 Actives by HPLC or GC |
12,500 |
Preliminary Analysis (OPPTS 830.1700)
| 1 Active by GC or HPLC |
10,100 |
| 1 Active by both GC and HPLC |
13,900 |
Characterization of an Active
| 1 Active by GC or HPLC, Active-GLP-C of A |
2,900 |
Storage
Both accelerated and low temperature storage conditions are offered as well as humidity controlled chambers.
Pharmaceutical Analysis
USP Monograph Testing
| Acid/Base Titration |
135 |
| Acetone (GC) |
155 |
| Acid Solubles or Insolubles |
145 |
| Acid Number |
145 |
| Acidity |
130 |
| Active Anionic |
160 |
| Alcohols (GC) |
155 – 180 |
| Alkaline Earths |
115 |
| Alkalinity |
140 |
| Amino Acids / Profile |
175 – 450 |
| Angular Rotation (specific rotation) |
155 |
| Appearance |
35 – 50 |
| Arsenic (USP) |
185 |
| Ash |
145 |
| Ash (Sulfated) |
155 |
| Barium (USP) |
95 |
| Benzalkonium Chloride |
170 |
| Benzethonium Chloride |
155 |
| Boiling Point |
180 |
| Bromide (USP) |
95 |
| Caffeine |
250 |
| Cetyl Pyridinium Chloride |
155 |
| Chloride (USP) |
85 |
| Chlorinated Compounds |
135 |
| Clarity of Solution (USP) |
100 |
| Cloud Point |
200 |
| Color (APHA) |
95 |
| Color of Solution |
95 |
| Completeness of Solution |
95 |
| Conductivity |
90 |
| Consistency (Petrolatum) |
310 |
| Degree of Polymerization |
215 |
| Density/Specific Gravity |
85 |
| Dextrose (HPLC) |
195 |
| Dextrins (USP) |
100 |
| Dissolution (Tablet/Capsule) |
1,000 – 1,800 |
| Dye Content |
150 |
| EDDI |
110 |
| EDTA Titration |
140 |
| Ether Soluble Substances |
140 |
| Ethylene Oxide, Propylene Oxide, Dioxane |
460 |
| Fatty Acids & Esters |
165 |
| Fatty Acid Profile (GC) |
275 – 400 |
| Ferrocyanides |
95 |
| Fixed Fats and Oils |
115 |
| Flash Point (Closed Cup) |
150 |
| Fluoride (ISE) |
125 |
| Folic Acid |
165 |
| Folin C |
285 |
| Formaldehyde |
155 |
| Free Fatty Acids |
130 |
| Freezing Point |
140 |
| FTIR |
155 |
| Glucosamine |
165 |
| Glycerin (GC) |
180 |
| Glycerin (HPLC/RI) |
200 |
| Glycerin ID B |
440 |
| Hardness (tablet) |
160 |
| Heavy Metals USP 231 |
225 |
| Heavy Metals USP 232 – No Validation |
1,050 – 1,250 |
| Heavy Metals USP 232 – Validation |
POR |
| Hydroxyl Value |
140 |
| Hylauronic Acid |
175 |
| Identification (IR/FTIR) |
155 – 200 |
| Identification (UV) |
155 – 170 |
| Insoluble Substances |
145 |
| Invert Sugar |
240 |
| Iodide (USP) |
110 |
| Iodine (Titration) |
110 – 130 |
| Iodine Value |
130 |
| Karl Fisher Water |
140 |
| Kjeldahl Nitrogen |
170 |
| Lead (USP) |
185 |
| Limit of Polycyclic Aromatics |
165 |
| Limit of Polynuclears |
165 |
| Loss on Drying |
140 |
| Melting Point |
150 |
| Metals/Minerals, Na, K, Ca, etc. |
120 |
| Methanol (GC) |
155 |
| Methoxy Groups |
410 |
| Molecular Weight Profile – Size Exclusion |
300 – 500 |
| Nitrate (USP) |
150 |
| Nitrite (USP) |
150 |
| Nitrogen (GC) |
170 |
| NMR |
POR |
| Non Volatile Residue |
145 |
| Organic Impurities (USP) |
370 – 600 |
| Oxygen (GC) |
170 |
| Pantothenol |
185 |
| Particle Size (Seive) |
130 |
| Peroxide Value |
155 |
| pH |
80 |
| Phosphorus |
120 |
| Polynuclear Aromatics |
165 |
| Povidone Idoine |
145 |
| Propylene Glycol (GC) |
185 |
| Propylene Glycol (HPLC-RI) |
200 |
| Propylene Glycol ID B |
460 |
| QUAT Compounds |
160 |
| Reducing Sugars |
160 |
| Refractive Index |
150 |
| Related Compounds (USP) |
375 – 600 |
| Residue on Ignition (USP) |
140 |
| Residual Solvents <467> |
950 -1,600 |
| Saponification Value |
150 |
| Silicon Dioxide |
160 |
| Sodium Hydroxide/Sodium Carbonate |
225 |
| Solids |
140 |
| Solid Parafin |
110 |
| Sorbitol |
195 |
| Spectinomycin |
260 |
| Stereochemical Purity (HPLC) |
350 – 500 |
| Sucralose |
195 |
| Sugar Profile (HPLC-RI) |
300 – 450 |
| Sulfate (USP) |
85 |
| Sulfide (USP) |
120 |
| Sulfur (HPLC) |
175 |
| Sulfur Dioxide (USP) |
360 |
| TLC |
250 – 350 |
| Total Organic Carbon (TOC) |
100 |
| Urea |
150 |
| Viscosity |
160 – 180 |
| Vitamin A (HPLC) |
190 |
| Vitamin D (HPLC) |
190 |
| Vitamin E (HPLC) |
190 |
| Vitamin B1 (HPLC) |
170 |
| Vitamin B2 (HPLC) |
160 |
| Vitamin B6 (HPLC) |
170 |
| Vitamin C (HPLC) |
155 |
| Water Soluble Substances |
140 |
Prices for multiple samples are negotiable.
Rush Charge additional 50% in 5 or fewer days.
Stability(Temperature/Humidity Controlled)
| Stability Storage Set-up/Lot |
150 – 200 |
| Monthly Storage Per Lot |
85 |
Assays / Purity
| Assay by Titration |
135 |
| Assay by Potentiometric Titration |
165 |
| Assay by HPLC (per active pharmaceutical or pesticide) – With 5-6 Standards Injections |
155 – 225 |
| Assay by GC (per active pharmaceutical or pesticide) – With 5-6 Standards Injections |
155 – 225 |
| Assay basic validation for specific product matrix – includes linearity, precision and spiked recovery |
950 – 1,750 |
| USP Standards |
USP Price + Shipping + Tax |
| Columns (HPLC or GC) Specific, specialized columns will be charged to the client with preapproval. |
|
| Method Development |
POR |
| Method Validation (USP parameters) |
POR |
| Method Verification |
POR |
| Method Transfer |
POR |
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